QuEChERS

The “QuEChERS” (Quick, Easy, Cheap, Effective, Rugged, and Safe) method, dispersive SPE (dSPE), is an emerging sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

In the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further clean up using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, clean up is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample clean up, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Details







AOAC 2007.01

Supelco carries a line of vials and centrifuge tubes containing pre-determine...(see detail)


EN 15662

PSA Tube, pk of 50, suitable for EN 15662:2008 per BS...(see detail)